Crystal structure of (R)-1-(1-(6-fluorobenzo[d]thiazol-2-yl)ethyl)-3-phenylthiourea
نویسندگان
چکیده
منابع مشابه
Crystal structure of (+)-(R)-3-methyl-1-(1'-phenyl-ethyl)-1H-pyridin-2-one.
wide interest because the 1H-pyridin-2-ones obtained in this process are versatile synthetic building blocks in the synthesis of alkaloids,1–5 although little has been done concerning their use in asymmetric synthesis. This contrasts with the large use of chiral piperidones, which have recently been reported. The synthetic method proceeds first through the addition of the hydroxide anion at pos...
متن کاملCrystal structure of (-)-(1'R)-1-(2'-hydroxy-1'-phenyl-ethyl)-1H-pyridin-2-one.
wide interest because the 1H-pyridin-2-ones obtained in this process are versatile synthetic building blocks in the synthesis of alkaloids.1–5 The title compound, (–)-(1′R)-1-(2′-hydroxy-1′-phenyl-ethyl)1H-pyridin-2-one II, was prepared by stirring a solution of pyridinium salt, I (4.0 mmol), in water (25 ml) and cooled to 5 ̊C (Scheme 1). A solution of K3Fe(CN)6 (11 eq.) in water (30 ml) was ad...
متن کاملCrystal structure of r-1,c-2-dibenzoyl-t-3,t-4-bis(2-nitrophenyl)cyclobutane
The condensation reaction of aceto-phenone (1-phenyl-ethan-1-one) with 2-nitro-benzaldehyde in the molten state yielded the expected chalcone, (E)-3-(2-nitro-phen-yl)-1-phenyl-prop-2-en-1-one, and, unexpectedly, the title compound, C30H22N2O6, which results from the syn head-to-head [2 + 2] cyclo-addition of the chalcone. The mol-ecular structure of the dimer shows that the four benzene rings o...
متن کاملCrystal structure of 3-(2-hydroxyethyl)-2-methylsulfanyl-6-nitro-3H-benzimidazol-1-ium chloride monohydrate
In the cation of the title hydrated molecular salt, C10H12N3O3S+·Cl-·H2O, the benzimidazolium ring system is almost planar (r.m.s. deviation = 0.006 Å) and the nitro group is inclined at an angle of 4.86 (9)° to this plane. In the crystal, C-H⋯O hydrogen bonds form centrosymmetric R22(20) dimers and these are further aggregated through N-H⋯O and O-H⋯Cl hydrogen bonds involving the water mol-ecu...
متن کاملCrystal structure of 1:1 complex crystal between 4-(3-methoxybenzyloxy)-6-methyl-2-pyrone and maleimide.
molecules are one of the important current topics because of unusual and interesting results.1,2 We have reported the solidstate [2+2]photocycloaddition reactions of 1:1 complex crystals between 2-pyrone derivatives and maleimide (2) to afford highly stereoselective cycloadducts.2 As a part of our continuing program, 1:1 complex crystal formation between 4(3-methoxybenzyloxy)-6-methyl-2-pyrone ...
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ژورنال
عنوان ژورنال: Zeitschrift für Kristallographie - New Crystal Structures
سال: 2016
ISSN: 2197-4578,1433-7266
DOI: 10.1515/ncrs-2015-0052